By V. G. Berezkin
During this two-part monograph, the writer describes smooth tools for the speedy column liquid chromatography of excessive- and medium-molecular-weight compounds of organic beginning, i.e. proteins, peptides, enzymes, nucleic acids, poly- and oligonucleotides, poly- and oligosaccharides, complicated biopolymers and biooligomers reminiscent of viruses, bacteriophages, ribosomes and glycoconjugates, in addition to another compounds reminiscent of immunomodulators. the cloth is contained in components: half A facing basic chromatographic conception, rules, fabrics and strategies; and half B facing the separation of person compound periods and containing a check in of chromatographed ingredients and a full-title bibliography. not just is that this a really expert, specific treatise on chromatographic innovations, it additionally offers a wide, balanced overview of swift separation of all recognized vital biopolymers and biooligomers, either uncomplicated and complicated, and in addition of a few synthetically ready and pharmaceutically very important biooligomers. additionally, it presents an advent to the appliance of HPLC to the research of the constitution of those ingredients.
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Additional info for Chemical Methods in Gas Chromatography
18. Device for the production of diazomethane. Reprinted with permission from ref. 100. C-H bond. As the methylenation reaction is not a selective reaction and the probability of methylene addition to different C-H bonds is determined only by their 'concentration' in the molecule of reacting hydrocarbon, the qualitative composition and the quantitative distribution of the products formed can be determined by calculation. , in the approximate ratio 6:4:2. Experimentally it was found that the products of n-pentane methylenation consist of 50% n-hexane, 34% 2-methylpentane and 16% 3-methylpentane , in full agreement with theory.
The ampoule can be heated for a long time so that the reaction is conducted at 650-7OO0C, and it breaks when the temperature is increased by a further 100-150°C. These limits can be changed by using glasses with different softening temperatures, Another interesting example of the application of the CFD method is the format'ion of volatile derivatives in the analysis of phosphates [ 1171 . Derivatives are formed in a PECULIARITIES OF THE ELABORATION OF TECHNIQUES i 43 + 5 Time (min I Fig. 22. Chromatograms of the products of chlorination of germanium ore with carbon tetrachloride.
The technique developed by Takahashi et al. [SO] makes it possible t o determine selectively and with high sensitivity the content of the above acids in blood, urine, etc. The limit of determination is 2 ng/ml for plasma and cerebrospinal fluid. ) packed with 2% OV-1 o n Chromosorb W. The cited examples are indicative of the necessity to estimate the duration of the CFD stage when developing the techniques for all compounds that are of analytical interest. Especially stringent requirements are placed on the rate of the chemical reactions used when the reaction proceeds in a chromatographic system, in a reactor before the column or at the beginning of the column.